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Low temperature ultraviolet and x ray photoelectron spectroscopy (LOTUS) - ARPES

Descrizione Descrizione
<p>The laboratory is devoted to the experimental investigation of the electronic band structure of surfaces and two-dim ensional (2D) materials by means of high-resolution angle-resolved ultraviolet photoelectron spectroscopy (ARPES). The ARPES apparatus, working at high energy and angle resolutions, operating at low temperatures, is contained into an ultra-high-vacuum (UHV) chamber, UHV-connected to a preparation chamber equipped withseveral other characterisation methods and ancillary facilities for samples preparation and 2D materials growth, and is provided with a small UHV chamber for a fast load-lock introduction chamber.</p>

<p>In the following, the main characteristics of the apparatus:</p>

<p>• ARPES hemispherical electron analyser: Scienta SES-200, 4 meV best energy resolution, &lt;0.1◦ angular resolution, 1-50 eV pass-energy range, multi-channel detector (MCD, ±8◦ angular span and 10% of pass-energy energy span);</p>

<p>• ARPES photon source: Omicron-Scienta VUV-5000 monochromatised MW-excited He source, main lines HeIα at 21.218 eV and HeIIα at 40.814 eV, up to HeIIδ at 52.241 eV;</p>

<p>• ARPES manipulator: 5-degrees of freedom UHV manipulator, with precision rotation of the azimuthal and polar angles, cryostat to liquid nitrogen temperature, electron-bombardment heater up to 1200◦C;</p>

<p>• Low-Energy Electron Diffraction (LEED): Specs retractable ErLEED system, with LEED and Auger modules;</p>

<p>• Ion Gun: Omicron ISE10 0.2-5 keV energy range, Ar ion source;</p>

<p>• Mass Spectrometer: residual gas analyser SRS RGA 300, 1-300 a.m.u. range;</p>

<p>• Gas line, equipped with several ports for small bottles and UHV-connected through a leak-valve to the main chamber; oxygen and C2H4 sources mounted, the latter for graphene preparation on metals via temperature programmed growth;</p>

<p>• Organic-molecular beam epitaxy (O-MBE) cells; high-temperature electron-bombardment based evaporator for transition metals; quartz crystal thickness monitor; cleaver, other ancillary facilities for sample preparation, etc.</p>

<p>Details at:</p>

<p><a href="https://drive.google.com/file/d/1h3-oAaZC7jxvg1d4j3Zhfrrl-A1-n2Hu/view">ARPES_laboratory.pdf - Google Drive</a></p>
Responsabile Responsabile
NomeE-mailStruttura
Carlo Mariani Carlo.Mariani@uniroma1.it DIPARTIMENTO DI FISICA
Dipartimento o centro ospitante Dipartimento o centro ospitante
DIPARTIMENTO DI FISICA
Attività Attività
  • Didattica 30 %
  • Ricerca 70 %
  • Servizio 0 %
ERC scientific sector ERC scientific sector
PE3_4PE3_10PE4_4
Keywords Keywords
2D nanostructures3D porous graphene
KET KET
Advanced materialsNanotecnologie
Personale docente e di ricerca Personale docente e di ricerca
NomeE-mailStruttura
Maria Grazia Betti mariagrazia.betti@uniroma1.it DIPARTIMENTO DI FISICA
Dario Marchiani dario.marchiani@uniroma1.it DIPARTIMENTO DI FISICA
Sunaina Rafiq sunaina.rafiq@uniroma1.it DIPARTIMENTO DI SCIENZE DI BASE ED APPLICATE PER L'INGEGNERIA
Sammar Tayyab tayyab.2025698@studenti.uniroma1.it DIPARTIMENTO DI SCIENZE DI BASE ED APPLICATE PER L'INGEGNERIA
Riccardo Frisenda riccardo.frisenda@uniroma1.it DIPARTIMENTO DI FISICA
Strumenti e attrezzature Strumenti e attrezzature
NomeDescrizioneServizi offerti
ARPESScienta SES-200 multichannel analyzer; Omicron-Scienta VUV-5000 monochromatised MW-excited He source; manipulator: 5-degrees of freedom UHV manipulator (heatbale and coolable sample holder); Low-Energy Electron Diffraction (LEED),Study of the band structure of ordered systems.
Printer
Computers
Ubicazione Ubicazione
Nome stanzaEdificioPiano
S17 CU013 -1

 


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bottom to top: manipulator, preparation chamber, analyzer and ARPES chamber
electron analyzer and UV source
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